Synthesis of 1-benzazepines as precursors of 1-benzazepinediones

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dc.contributor.authorPessoa Mahana, H
dc.contributor.authorValderrama, JA
dc.date.accessioned2024-01-10T12:43:19Z
dc.date.available2024-01-10T12:43:19Z
dc.date.issued2000
dc.description.abstractThe synthesis of 6-hydroxy-7-nitro-1-benzazepine-2-one 7 from 5-hydroxy-1 -tetralone 1 and 6-hydroxy-1 -benzazepine-2-one 2 is described. Bromination of 6-hydroxy- 1-benzazepine-2-one 2 with NBS in ethyl acetate afforded 7-bromo-6-hydroxy-1 -benzazepine-2-one 13 and 7,9-dibromo-6-hydroxy-1-benzazepine-2-one 14. Oxidation of benzazepinone 13 with (diacetoxyiodo)benzene provided 7-bromo-1-benzazepine-2,6,9-trione 5.
dc.fechaingreso.objetodigital2024-05-06
dc.format.extent10 páginas
dc.fuente.origenWOS
dc.identifier.doi10.1080/00397910008087260
dc.identifier.issn0039-7911
dc.identifier.urihttps://doi.org/10.1080/00397910008087260
dc.identifier.urihttps://repositorio.uc.cl/handle/11534/77585
dc.identifier.wosidWOS:000088919700001
dc.information.autorucQuímica;Valderrama J;S/I;98772
dc.issue.numero19
dc.language.isoen
dc.nota.accesocontenido parcial
dc.pagina.final3490
dc.pagina.inicio3481
dc.publisherMARCEL DEKKER INC
dc.revistaSYNTHETIC COMMUNICATIONS
dc.rightsacceso restringido
dc.subjectBROMONAPHTHOQUINONES
dc.subjectQUINONES
dc.subject.ods03 Good Health and Well-being
dc.subject.odspa03 Salud y bienestar
dc.titleSynthesis of 1-benzazepines as precursors of 1-benzazepinediones
dc.typeartículo
dc.volumen30
sipa.codpersvinculados98772
sipa.indexWOS
sipa.indexScopus
sipa.trazabilidadCarga SIPA;09-01-2024
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